Test Specification Min Max ASSAY APPROX. 97 % APPROX. 97 %

Test Specification Min Max APPEARANCE WHITE-OFF-WHITE WHITE-OFF-WHITE DL-alpha-TOCOPHERYL ACETATE 74% 74% PARTICLE SIZE 99 % (< 20 MESH) 99 % (< 20 MESH) LOSS ON DRYING 3% EXPIRATION DATE

Test Specification Min Max ASSAY 99.00% 99.00% RETEST DATE

Test Specification Min Max APPEARANCE WHITE,CRYSTALLIN WHITE,CRYSTALLIN ODOR SLIGHT CHARACTER SLIGHT CHARACTER ASSAY (DRIED BASIS) 99.0 - 101.0% 99.0 - 101.0% MELTING RANGE 168� - 172�C 168� - 172�C pH...

Test Specification Min Max ASSAY (DRIED BASIS) 99.0 - 101.0 % 99.0 - 101.0 % ACIDITY TO PASS TEST TO PASS TEST HEAVY METALS 20 ppm LOSS ON DRYING 0.50%...

Test Specification Min Max ASSAY 94% 94% MELTING POINT 131 - 134 C 131 - 134 C

Test Specification Min Max ASSAY (Na[@2@]O[@2@]) 93.00% 93.00% CHLORIDE (Cl) 0.00% PHOSPHATE (PO[@4@]) 5 ppm SULFATE 0.00% HEAVY METALS (as Pb) 0.00% IRON (Fe) 0.01% EXPIRATION DATE

Test Specification Min Max APPEARANCE

Test Specification Min Max APPEARANCE FAINT YELLOW TO FAINT YELLOW TO CLARITY CLEAR TO VERY SL CLEAR TO VERY SL IODINE VALUE 103 - 112 103 - 112 GLC DETERMINATION...

Test Specification Min Max ASSAY (Na[@2@]CO[@3@]; DRY BASIS) 99.5 100.50% LEAD (Pb) 4 mg/kg LOSS ON DRYING 1% IDENTIFICATION TO PASS TEST

Test Specification Min Max ASSAY 98% SPECIFIC GRAVITY @ 20/20 C 0.813 0.818 ACIDITY 0.03% METHYL ETHYL KETONE 0.20% WATER 0.50%

Test Specification Min Max ASSAY (K[@2@]SO[@4@]) 99 100.50% LEAD (Pb) 2 mg/kg SELENIUM (Se) 5 mg/kg IDENTIFICATION TO PASS TEST TO PASS TEST RETEST DATE DATE OF MANUFACTURE APPEARANCE

Test Specification Min Max ASSAY 99% 99%

Test Specification Min Max TOTAL CAPSAICINOIDS 90 110.00% CAPSAICIN (C[@18@]H[@27@]NO[@3@]) 55% DIHYDROCAPSAICIN (C[@18@]H[@29@]NO[@3@]) 20% MELTING RANGE 57� 66�C LOSS ON DRYING 1.00% OTHER CAPSAICINOIDS 15% RESIDUE ON IGNITION 1.00% ELEMENTAL...

Test Specification Min Max ASSAY 98% 98%

Test Specification Min Max PURITY (by TLC) ONE SPOT ONE SPOT ABSORBANCE OF A 5% SOLUTION @ 300 nm 0.1 A.U

Test Specification Min Max ASSAY 99% 99%

Test Specification Min Max ASSAY APPROX. 99 % APPROX. 99 %

Test Specification Min Max ASSAY 98% RETEST DATE

Test Specification Min Max ASSAY (DRIED BASIS) 98.00% MOISTURE 8.00%

Test Specification Min Max WEIGHT AVERAGE MOLECULAR WEIGHT 35,000 45,000 NUMBER AVERAGE MOLECULAR WEIGHT 16,000 30,000 SPECIFIC ROTATION +195� to +203� +195� to +203� SAFETY TO PASS TEST TO PASS...

CAS #: 75-60-5   Test Specification Min Max ASSAY 99.00% 99.00%

Test Specification Min Max ASSAY (HPLC) 97 102.00% EXPIRATION DATE

Test Specification Min Max ACTIVITY 10% 10% LOSS ON DRYING 8% MICROBIAL LIMITS: ESCHERICHIA COLI 10 CFU/g SALMONELLA NEGATIVE EXPIRATION DATE

Test Specification Min Max ASSAY 99.00% 99.00%

Test Specification Min Max ASSAY 98% WATER 0.25% RESIDUE ON IGNITION 0.05% RETEST DATE

Test Specification Min Max ASSAY 99.00% INSOLUBLE MATTER 0.01% ALKALINITY TO PASS TEST TO PASS TEST TITRABLE ACID 0.035 meq/ CHLORIDE (Cl) 0.00% SULFATE 0.01% BARIUM 0.01% HEAVY METALS (as...

Test Specification Min Max APPEARANCE

Test Specification Min Max ASSAY 99.00% 99.00%

Test Specification Min Max ASSAY [Bi(NO[@3@])[@3@][-5H[@2@]O] 98.00% INSOLUBLE MATTER 0.01% CHLORIDE (Cl) 0.00% SULFATES (SO[@4@]) 0.01% ARSENIC (As) 0.00% COPPER (Cu) 0.00% IRON (Fe) 0.00% LEAD (Pb) 0.00% SILVER (Ag)...

Test Specification Min Max ASSAY (DRIED BASIS) 95.00% MELTING RANGE 107� 117�C SPECIFIC ROTATION (C=10 ; METHANOL) +21� to +24� +21� to +24� LEAD (Pb) 2 mg/kg LOSS ON DRYING...

Test Specification Min Max APPEARANCE

Test Specification Min Max APPEARANCE TO PASS TEST TO PASS TEST GEL TEMPERATURE (1.5%) 36 - 39 C 36 - 39 C EEO 0.1 SULFATE 0.30% ASH 0.50% MOISTURE 10.00%...

Test Specification Min Max ASSAY [(CH[@3@]CO)[@2@]O] 97.00% RESIDUE AFTER EVAPORATION 0.00% CHLORIDE (Cl) 5 ppm PHOSPHATE (PO[@4@]) 0.00% SULFATES (SO[@4@]) 5 ppm HEAVY METALS (as Pb) 2 ppm IRON (Fe)...

Test Specification Min Max ASSAY (ANHYDROUS BASIS) 98.5 101.00% CHROMATOGRAPHIC PURITY TO PASS TEST WATER DETERMINATION 0.50% RESIDUE ON IGNITION 0.10% ELEMENTAL IMPURITIES AS REPORTED AS REPORTED IDENTIFICATION TO PASS...

Test Specification Min Max APPEARANCE